Agilent Technologies 1290 Infinity II Bedienungsanleitung

Agilent Technologies

Agilent 1290 Infinity II

Variable Wavelength

Detector

User Manual

Agilent 1290 Infinity II VWD User Manual

Notices

No part of this manual may be reproduced

in any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G7114-90000 Rev. B

Edition

12/2014

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

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The material contained in this docu-

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in future editions. Further, to the max-

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Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

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or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

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met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

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Agilent 1290 Infinity II VWD User Manual 3

In This Book

This manual covers the Agilent 1290 Infinity II Variable Wavelength

Detector (G7114B).

Find information on other Agilent Variable Wavelength Detectors in

separate manuals.

1 Introduction to the Variable Wavelength Detector

This chapter gives an introduction to the detector, instrument overview

and internal connectors.

2 Site Requirements and Specifications

This chapter gives information on environmental requirements, physical

and performance specifications.

3 Using the Module

This chapter explains the essential operational parameters of the module.

4 Preparing the Module

This chapter provides information on how to set up the detector for an

analysis and explains the basic settings.

5 Optimizing the Detector

This chapter provides information on how to optimize the detector.

6 Troubleshooting and Diagnostics

Overview about the troubleshooting and diagnostic features.

7 Error Information

This chapter describes the meaning of detector error messages, and

provides information on probable causes and suggested actions how to

recover from error conditions.

4 Agilent 1290 Infinity II VWD User Manual

In This Book

8TestFunctions

This chapter describes the detector’s built in test functions.

9 Maintenance

This chapter provides general information on maintenance of the detector.

10 Parts and Materials for Maintenance

This chapter provides information on parts for maintenance.

11 Identifying Cables

This chapter provides information on cables used with the Agilent 1200

Infinity Series modules.

12 Hardware Information

This chapter describes the detector in more detail on hardware and

electronics.

13 LAN Configuration

This chapter provides information on connecting the module to the Agilent

ChemStation PC.

14 Appendix

This chapter provides addition information on safety, legal and web.

Agilent 1290 Infinity II VWD User Manual 5

Contents

1 Introduction to the Variable Wavelength Detector 9

Introduction to the Detector 10

Product Description 11

Optical System Overview 12

Dual-Wavelength Mode 17

Leak and Waste Handling 18

Operating Principle 21

2 Site Requirements and Specifications 23

Site Requirements 24

Physical Specifications 27

Performance Specifications G7114B 28

3 Using the Module 31

Magnets 32

Turn on/off 33

Status Indicators 34

Instrument Configuration 35

Set up the Detector with Agilent Open Lab ChemStation 37

The Detector User Interface 38

Detector Control Settings 40

Method Parameter Settings 41

Scanning with the VWD 45

4 Preparing the Module 47

Leak and Waste Handling 48

Setting up an Analysis 50

Solvent Information 57

6 Agilent 1290 Infinity II VWD User Manual

Contents

5 Optimizing the Detector 63

Introduction 64

Match the Flow Cell to the Column 65

Set the Detector Parameters 68

Warm up of the Detector 69

6 Troubleshooting and Diagnostics 71

Available Tests versus Interfaces 72

Agilent Lab Advisor Software 73

7 Error Information 75

What Are Error Messages 77

General Error Messages 78

Detector Error Messages 85

8TestFunctions 95

Introduction 96

Intensity Test 97

Cell Test 100

Wavelength Verification-Calibration 102

ASTM Drift and Noise Test 104

Quick Noise Test 105

Dark Current Test 107

Holmium Oxide Test 109

D/A Converter (DAC) Test 112

Other Lab Advisor Functions 115

9 Maintenance 117

Introduction to Maintenance 118

Warnings and Cautions 118

Overview of Maintenance 120

Cleaning the Module 121

Remove and Install the Doors 122

Replace the Deuterium Lamp 123

Replace the Flow Cell / Cuvette Holder 126

Repairing the Flow Cells 128

Agilent 1290 Infinity II VWD User Manual 7

Contents

Using the Cuvette Holder 131

Correcting Leaks 133

Replacing Leak Handling System Parts 135

Replace the Module Firmware 136

10 Parts and Materials for Maintenance 139

Overview of Maintenance Parts 140

Standard Flow Cell 10 mm / 14 µL 142

Micro Flow Cell 3 mm / 2 µL 144

Semi-micro Flow Cell 6 mm / 5 µL 146

High Pressure Flow Cell 10 mm / 14 µL 148

Cuvette Holder 150

Accessory Kit 151

11 Identifying Cables 153

Cable Overview 154

Analog Cables 156

Remote Cables 158

CAN/LAN Cables 162

RS-232 Cables 163

USB Cables 164

12 Hardware Information 165

Firmware Description 166

Electrical Connections 169

Interfaces 172

Setting the 6-bit Configuration Switch 179

Instrument Layout 183

Early Maintenance Feedback 184

8 Agilent 1290 Infinity II VWD User Manual

Contents

13 LAN Configuration 187

What You Have to Do First 188

TCP/IP parameter configuration 189

Configuration Switch 190

Initialization Mode Selection 191

Dynamic Host Configuration Protocol (DHCP) 195

Manual Configuration 198

PC and Agilent ChemStation Setup 202

14 Appendix 211

General Safety Information 212

Waste Electrical and Electronic Equipment Directive 220

Radio Interference 221

Sound Emission 222

Solvent Information 223

Declaration of Conformity for HOX2 Filter 224

Agilent Technologies on Internet 225

Agilent 1290 Infinity II VWD User Manual

Agilent Technologies

Introduction to the Variable Wavelength

Detector

Introduction to the Detector 10

Product Description 11

Optical System Overview 12

Flow Cell 13

Lamp 14

Source Lens Assembly 14

Entrance Slit Assembly 14

Filter Assembly 15

Mirror Assemblies M1 and M2 16

Grating Assembly 16

Beam Splitter Assembly 16

Photo Diodes Assemblies 16

Photo Diode ADC (analog-to-digital converter) 16

Dual-Wavelength Mode 17

Leak and Waste Handling 18

Waste Concept 20

Operating Principle 21

This chapter gives an introduction to the detector, instrument overview and

internal connectors.

10 Agilent 1290 Infinity II VWD User Manual

1Introduction to the Variable Wavelength Detector

Introduction to the Detector

The Agilent variable wavelength detectors described in this manual are

designed for highest optical performance, GLP compliance and easy

maintenance with:

•higher data rate up to 240 Hz for ultra- fast- HPLC (G7114B),

•deuterium lamp for highest intensity and lowest detection limit over a

wavelength range of 190 to 600 nm,

•optional flow- cell cartridges (standard 10 mm, 14 µL; high pressure

10 mm, 14 µL; micro 3 mm, 2 µL; semi- micro 6 mm, 5 µL) and Prep

Cells are available and can be used depending on the application needs

(other types may be introduced later),

•Dual wavelength mode, see “Dual- Wavelength Mode” on page 17.

•easy front access to lamp and flow cell for fast replacement,

•electronic identification of flow cell and lamp with RFID (Radio

Frequency Identification) tag for unambiguous identification,

•lamp information: part number, serial number, production date,

ignitions, burn time

•cell information: part number, serial number, production date,

nominal path length, volume, maximum pressure

•built- in electronic temperature control (ETC) for improved baseline

stability, and

•built- in holmium oxide filter for fast wavelength accuracy verification.

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