Agilent Technologies 1290 infinity Bedienungsanleitung

Agilent Technologies

Agilent 1290 Infinity

Quaternary Pump

User Manual

1290 Infinity Quaternary Pump User Manual

Notices

2015

No part of this manual may be reproduced

in any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G4204-90000 Rev. F

Edition

02/2015

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or perfor-

mance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a license

and may be used or copied only in accor-

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Restricted Rights Legend

If software is for use in the performance of a

U.S. Government prime contract or subcon-

tract, Software is delivered and licensed as

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or as a “commercial item” as defined in FAR

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ware” as defined in FAR 52.227-19 (June

1987) or any equivalent agency regulation

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closure of Software is subject to Agilent

Technologies’ standard commercial license

terms, and non-DOD Departments and

Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully under-

stood and met.

1290 Infinity Quaternary Pump User Manual 3

In This Guide...

This manual covers the Agilent 1290 Infinity Quaternary Pump (G4204A).

1 Introduction

This chapter gives an introduction to the module, instrument overview and

internal connectors.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical

and performance specifications.

3 Installing the Module

This chapter gives information about the preferred stack setup for your

system and the installation of your Agilent 1290 Infinity Quaternary

Pump.

4UsingthePump

This chapter explains the operational parameters of the Agilent 1290

Infinity Quaternary Pump.

5 How to Optimize the Performance of Your Module

This chapter gives hints on how to optimize the performance or use

additional devices.

6 Troubleshooting and Diagnostics

Overview about the troubleshooting and diagnostic features.

7 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

4 1290 Infinity Quaternary Pump User Manual

In This Guide...

8 Test Functions and Calibrations

This chapter will describe the tests for the module.

9 Maintenance

This chapter describes the maintenance of the Agilent 1290 Infinity

Quaternary Pump.

10 Parts and Materials

This chapter provides information on parts for maintenance.

11 Identifying Cables

This chapter provides information on cables used with the Agilent 1200

Infinity Series modules.

12 Hardware Information

This chapter describes the pump in more detail on hardware and

electronics.

13 LAN Configuration

This chapter provides information on connecting the module to the

controller software.

14 Appendix

This chapter provides additional information on safety, legal and web.

1290 Infinity Quaternary Pump User Manual 5

Contents

1 Introduction 9

Features 10

Overview of the Quaternary Pump 11

Operating Principle 12

Positions of the Multi Purpose Valve 14

System Overview 19

2 Site Requirements and Specifications 23

Site Requirements 24

Physical Specifications 27

Performance Specifications 28

3 Installing the Module 31

Unpacking the Module 32

Optimizing the Stack Configuration 34

Installation Information on Leak and Waste Handling 39

Removing the Transport Foam 43

Installing the Pump 44

Flow Connections to the Pump 46

Installation of Seal Wash Option 49

4UsingthePump 51

Leak and Waste Handling 52

Preparing the Pump 53

Algae Growth in HPLC Systems 54

Setting up the Pump with the Instrument Control Interface 55

Priming the Pump 68

Flushing the Filter 70

Solvent Information 72

6 1290 Infinity Quaternary Pump User Manual

Contents

5 How to Optimize the Performance of Your Module 79

Using the Degasser 80

Operational Hints for the Multi Channel Gradient Valve (MCGV) 81

Delay Volume and Extra-Column Volume 82

How to Configure the Optimum Delay Volume 83

How to Achieve Higher Resolution 85

Using Solvent Calibration Tables 88

6 Troubleshooting and Diagnostics 89

Overview of the Module’s Indicators and Test Functions 90

Status indicators 91

Available Tests vs User Interfaces 93

Agilent Lab Advisor Software 94

7 Error Information 95

What Are Error Messages 97

General Error Messages 98

Pump Error Messages 103

8 Test Functions and Calibrations 121

9 Maintenance 123

Introduction to Maintenance 125

Warnings and Cautions 126

Overview of Maintenance 128

Cleaning the Module 129

Installing Fittings and Capillaries 130

Replacing the Pressure Sensor 131

Replacing the Inlet Weaver 134

Replacing the Inlet Valve 136

Replacing the Outlet Valve 137

Removing the Jet Weaver 139

Installing the Jet Weaver 141

Replacing the Seal Wash Pump 143

Replacing the Multi-Channel Gradient Valve (MCGV) 145

Releasing a Stuck Inlet Valve 149

Replacing the Pump Head 152

1290 Infinity Quaternary Pump User Manual 7

Contents

Disassembling the Pump Head 158

Disassembling the Primary Pump Head 160

Disassembling the Secondary Pump Head 164

Replacing the Heat Exchanger 168

Replacing Wash Seal and Gasket 171

Assembling the Pump Head 173

Replacing the Multi Purpose Valve 185

Replacing Parts of the Multi Purpose Valve 188

Replacing the Outlet Filter 189

Replacing Parts of the Inline Filter 191

Installing the Valve Rail Kit 194

Replacing Module Firmware 195

Preparing the Pump Module for Transport 196

10 Parts and Materials 201

Overview of Main Assemblies 202

Flow Connections 204

Seal Wash Option 206

Pump Head Assembly Parts 207

Primary Pump Head Parts 208

Secondary Pump Head Parts 212

Multi Purpose Valve 216

Solvent Cabinet 218

Cover Parts 220

Leak Parts 222

Accessory Kit 224

Others 225

11 Identifying Cables 227

Cable Overview 228

Analog cables 230

Remote Cables 232

BCD Cables 235

CAN/LAN Cable 237

RS-232 Cable Kit 238

Agilent 1200 Module to Printer 239

8 1290 Infinity Quaternary Pump User Manual

Contents

12 Hardware Information 241

Firmware Description 242

Electrical Connections 245

Interfaces 247

Setting the 8-bit Configuration Switch 254

Early Maintenance Feedback 257

Instrument Layout 258

13 LAN Configuration 259

What You Have To Do First 260

TCP/IP Parameter Configuration 261

Configuration Switch 262

Initialization Mode Selection 263

Dynamic Host Configuration Protocol (DHCP) 267

Link Configuration Selection 270

Automatic configuration with Bootp 271

Manual Configuration 281

PC and User Interface Software Setup Setup 287

14 Appendix 289

General Safety Information 290

The Waste Electrical and Electronic Equipment (WEEE) Directive

(2002-96-EC) 293

Radio Interference 294

Sound Emission 295

Agilent Technologies on Internet 296

1290 Infinity Quaternary Pump User Manual

Agilent Technologies

Introduction

Features 10

Overview of the Quaternary Pump 11

Operating Principle 12

Positions of the Multi Purpose Valve 14

System Overview 19

Leak and Waste Handling 19

This chapter gives an introduction to the module, instrument overview and

internal connectors.

10 1290 Infinity Quaternary Pump User Manual

1Introduction

Features

The G4204A Quaternary Pump is designed for highest performance, GLP

compliance and easy maintenance. It includes the following features:

•Optional seal wash for continued high lifetime of pump seals for buffer

applications.

•Optional Jet Weaver for optimum mixing performance with a minimum

of delay volume.

•Automatic purge function for ease of use and unattended preparation of

the system.

•Auto tuning of the delivery cycle for compensation of elasticity and

solvent volume change effects (compressibility, thermal expansion).

•Solvent selection for optimum flow accuracy.

•Fast defill function for improved intake and delivery performance.

•Two pistons in series design for increased reliability.

•High resolution piston movement control for smooth and reliable

motion.

For specifications, see “Performance Specifications” on page 28.

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