Agilent Technologies LC Series Bedienungsanleitung

Agilent Technologies

Agilent InfinityLab LC Series

1260 Infinity II Isocratic-

and Quaternary Pumps

User Manual

Agilent InfinityLab LC Series 1260 Infinity II Isocratic- and Quaternary Pumps User Manual

Notices

No part of this manual may be reproduced

in any form or by any means (including

electronic storage and retrieval or transla-

tion into a foreign language) without prior

agreement and written consent from Agi-

lent Technologies, Inc. as governed by

United States and international copyright

laws.

Manual Part Number

G7111-90000 Rev. C

Edition

08/2018

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or perfor-

mance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a

license and may be used or copied only in

accordance with the terms of such license.

Restricted Rights Legend

If software is for use in the performance of

a U.S. Government prime contract or sub-

contract, Software is delivered and licensed

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or as a “commercial item” as defined in

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software” as defined in FAR 52.227-19

(June 1987) or any equivalent agency regu-

lation or contract clause. Use, duplication

or disclosure of Software is subject to Agi-

lent Technologies’ standard commercial

license terms, and non-DOD Departments

and Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully

understood and met.

Agilent InfinityLab LC Series 1260 Infinity II Isocratic- and Quaternary Pumps User Manual 3

In This Guide...

This manual covers:

•Agilent 1260 Infinity II Isocratic Pump (G7110B),

•Agilent 1260 Infinity II Quaternary Pump VL (G7111A),

•Agilent 1260 Infinity II Quaternary Pump (G7111B), and

•Agilent 1260 Infinity II Bio-inert Pump (G5654A).

1Introduction

This chapter gives an introduction to the module, instrument overview and

internal connectors.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical

and performance specifications.

3UsingthePump

This chapter provides information for optimized usage of the module.

4 Optimizing Performance

This chapter gives hints on how to optimize the performance or use additional

devices.

5 Troubleshooting and Diagnostics

This chapter gives an overview about the troubleshooting and diagnostic

features and the different user interfaces.

6 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

4 Agilent InfinityLab LC Series 1260 Infinity II Isocratic- and Quaternary Pumps User Manual

In This Guide...

7 Test Functions and Calibration

This chapter describes the tests for the module.

8 Maintenance

This chapter describes the maintenance of the module.

9PartsforMaintenance

This chapter provides information on parts for maintenance.

10 Identifying Cables

This chapter provides information on cables used with the Agilent 1200

Infinity Series modules.

11 Hardware Information

This chapter describes the pump in more detail on hardware and electronics.

12 LAN Configuration

This chapter provides information on connecting the module to the Agilent

ChemStation PC.

13 Appendix

This chapter provides addition information on safety, legal and web.

Agilent InfinityLab LC Series 1260 Infinity II Isocratic- and Quaternary Pumps User Manual 5

Contents

1Introduction 9

Introduction to the Pump 10

G7110B Isocratic Pump 11

G7111A Quaternary Pump VL 13

G7111B Quaternary Pump 15

G5654A Bio-inert Pump 17

Overview of the Hydraulic Path 19

Leak and Waste Handling 27

2 Site Requirements and Specifications 33

Site Requirements 34

Physical Specifications 37

Performance Specifications 41

3UsingthePump 49

Magnets 50

Turn on/off 51

Status Indicators 53

Best Practices 54

Leak and Waste Handling 57

Hints for Successful Use of the Pump 59

Setting up the Pump with the G4208A Instant Pilot 60

Setting up the Pump with the Instrument Control Interface 61

Solvent Information 71

Algae Growth in HPLC Systems 81

Prevent Blocking of Solvent Filters 82

Normal Phase Applications 83

4 Optimizing Performance 85

Using the Degasser 86

Operational Hints for the Vacuum Degasser 87

Operational Hints for the Multi Channel Gradient Valve (MCGV) 88

When to use the Seal Wash Function 89

Choosing the Right Pump Seals 90

Optimize the Compressibility Compensation Setting 91

6 Agilent InfinityLab LC Series 1260 Infinity II Isocratic- and Quaternary Pumps User Manual

Contents

5 Troubleshooting and Diagnostics 93

User Interfaces 94

Agilent Lab Advisor Software 95

6 Error Information 97

What Are Error Messages 99

General Error Messages 100

Module Error Messages 106

7 Test Functions and Calibration 121

Introduction 122

System Pressure Test 123

Leak Rate Test 128

8 Maintenance 135

Introduction to Maintenance and Repair 136

Warnings and Cautions 137

Overview of Maintenance and Repair 138

Cleaning the Module 139

Remove and Install Doors 140

Checking and Replacing the Solvent Filter 141

Exchange the Passive Inlet Valve 142

Exchange the Outlet Valve 144

Exchange the Purge Valve Frit or the Purge Valve 146

Replace the O-Ring on the Purge Valve 150

Remove the Pump Head Assembly 153

Maintenance of a Pump Head Without Seal Wash Option 155

Maintenance of a Pump Head with Seal Wash Option 158

Reinstall the Pump Head Assembly 162

Seal Wear-in Procedure 165

Exchange the Multi-Channel Gradient Valve (MCGV) 166

Replace the Solvent Selection Valve (Isocratic Pump) 169

Exchange the Active Inlet Valve (AIV) or its Cartridge 171

Exchange the Seal Wash Cartridge 173

Replace Leak Handling System Parts 174

Replacing the Module Firmware 175

Agilent InfinityLab LC Series 1260 Infinity II Isocratic- and Quaternary Pumps User Manual 7

Contents

9 Parts for Maintenance 177

Accessory Kits 178

Pump Head Assembly Without Seal Wash 180

Pump Head Assembly with Seal Wash Option 182

Outlet Valve 185

Purge Valve Assembly 186

Active Inlet Valve Assembly 188

1260 Infinity II Max Uptime Kit 190

1260 Infinity II Max Uptime Kit Bio 191

1260 Infinity II Low Dispersion Kit MCT 192

HPLC System Tool Kit 193

Solvent Cabinet 194

Bottle Head Assembly 195

Hydraulic Path of the Quaternary Pump 196

Hydraulic Path of the Isocratic Pump 198

10 Identifying Cables 201

Cable Overview 202

Analog Cables 204

Remote Cables 206

CAN Cable 210

Agilent Module to PC 211

Agilent 1200 Module to Printer 212

11 Hardware Information 213

Firmware Description 214

Electrical Connections 217

Interfaces 219

Setting the 6-bit Configuration Switch 227

Instrument Layout 231

Early Maintenance Feedback 232

12 LAN Configuration 233

What You Have to Do First 234

TCP/IP parameter configuration 235

Configuration Switches 236

Initialization Mode Selection 237

Dynamic Host Configuration Protocol (DHCP) 239

Manual Configuration 242

8 Agilent InfinityLab LC Series 1260 Infinity II Isocratic- and Quaternary Pumps User Manual

Contents

13 Appendix 247

General Safety Information 248

Waste Electrical and Electronic Equipment (WEE) Directive 254

Radio Interference 255

Sound Emission 256

Agilent Technologies on Internet 257

Agilent InfinityLab LC Series 1260 Infinity II Isocratic- and Quaternary

Pumps User Manual

Agilent Technologies

Introduction

Introduction to the Pump 10

G7110B Isocratic Pump 11

Product Description 11

Features 12

G7111A Quaternary Pump VL 13

Product Description 13

Features 14

G7111B Quaternary Pump 15

Product Description 15

Features 16

G5654A Bio-inert Pump 17

Product Description 17

Features 18

Overview of the Hydraulic Path 19

Hydraulic Path 20

How Does the Pump Work? 22

How Does Compressibility Compensation Work? 25

How Does Variable Stroke Volume Work? 26

Leak and Waste Handling 27

Leak Sensor 31

Waste Concept 31

This chapter gives an introduction to the module, instrument overview and

internal connectors.

10 Agilent InfinityLab LC Series 1260 Infinity II Isocratic- and Quaternary Pumps User Manual

Introduction

Introduction to the Pump

The Pumps comprise one pump head unit with an optional solvent cabinet, a

vacuum degasser (optional for the isocratic pump), and a multi-channel

gradient valve (MCGV) for quaternary pumps, or an optional solvent selection

valve (SSV) for isocratic pumps. The combination of the pump head assembly

and high speed proportioning MCGV with a possible connection up to four

different solvents in quaternary pumps provides gradient generation by low

pressure mixing. The combination of the pump head assembly and SSV in

isocratic pump provides opportunity to make a choice between three different

solvents. A solvent cabinet provides enough space for eight one-liter bottles.

The Active Seal Wash (ASW) and Active Inlet Valve (AIV) options are available

for quaternary pumps when concentrated buffer solutions are used. The

Bio-inert pump is optimized for these conditions, thus is always equipped with

ASW and AIV.

Figure 1 Overview of the pump

'HJDVVHU

0&*9

,QOHW9DOYH

2XWOHW9DOYH

3XPS+HDG

3XUJH9DOYH

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